ISO 6721-10-1999 塑料动态机械性能的测定第10部分:使用平板振荡流变仪测定复合剪切粘度
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【英文标准名称】:Plastics-Determinationofdynamicmechanicalproperties-Part10:Complexshearviscosityusingaparallel-plateoscillatoryrheometer
【原文标准名称】:塑料动态机械性能的测定第10部分:使用平板振荡流变仪测定复合剪切粘度
【标准号】:ISO6721-10-1999
【标准状态】:现行
【国别】:国际
【发布日期】:1999-12
【实施或试行日期】:
【发布单位】:国际标准化组织(IX-ISO)
【起草单位】:ISO/TC61
【标准类型】:()
【标准水平】:()
【中文主题词】:机械性能;测定;试验;定义;高聚物熔化;高聚物;塑料;振荡器;流变测定法;粘度测量;剪切模量;动态试验
【英文主题词】:Definition;Definitions;Determination;Dynamictesting;Mechanicalproperties;Oscillators;Plastics;Polymermelt;Polymers;Rheometry;Shearmodulus;Testing;Viscositymeasurement
【摘要】:ThispartofISO6721specifiesthegeneralprinciplesofamethodfordeterminingthedynamicrheologicalpropertiesofpolymermeltsatangularfrequenciestypicallyintherange0,01rad·sto100rad·sbymeansofanoscillatoryrheometerwithaparallel-plategeometry.Angularfrequenciesoutsidethisrangecanalsobeused(seenote1).Themethodisusedtodeterminevaluesofthefollowingdynamicrheologicalproperties:complexshearviscosityη,dynamicshearviscosityη',theout-of-phasecomponentofthecomplexshearviscosityη",complexshearmodulusG,shearlossmodulusG"andshearstoragemodulusG'.Itissuitableformeasuringcomplexshearviscosityvaluestypicallyuptoapproximately10MPa·s(seenote2).NOTE1Theangular-frequencymeasurementrangeislimitedbythespecificationofthemeasuringinstrumentandalsobytheresponseofthespecimen.Whentestingusingangularfrequencieslowerthan0,1rad·sthetesttimecanincreasesignificantlyasthetimetakentoobtainasinglemeasurementisproportionaltothereciprocaloftheangularfrequency.Consequently,whentestingatlowangularfrequenciesdegradationorpolymerizationofthespecimenismorelikelytooccurandhaveaneffectontheresults.Athighangularfrequenciesthespecimenmaydistortorfractureattheedge,consequentlyinvalidatingthetestresults.NOTE2Therangeofcomplexshearviscosityvaluesthatcanbemeasuredisdependentonthespecimendimensionsandalsothespecificationofthemeasuringinstrument.Foraspecimenofgivendimensions,theupperlimitoftherangeislimitedbythemachine'storquecapacity,angular-displacementresolutionandcompliance.However,correctioncanbemadeforcomplianceeffects.
【中国标准分类号】:G31
【国际标准分类号】:83_080_01
【页数】:15P.;A4
【正文语种】:英语
【原文标准名称】:塑料动态机械性能的测定第10部分:使用平板振荡流变仪测定复合剪切粘度
【标准号】:ISO6721-10-1999
【标准状态】:现行
【国别】:国际
【发布日期】:1999-12
【实施或试行日期】:
【发布单位】:国际标准化组织(IX-ISO)
【起草单位】:ISO/TC61
【标准类型】:()
【标准水平】:()
【中文主题词】:机械性能;测定;试验;定义;高聚物熔化;高聚物;塑料;振荡器;流变测定法;粘度测量;剪切模量;动态试验
【英文主题词】:Definition;Definitions;Determination;Dynamictesting;Mechanicalproperties;Oscillators;Plastics;Polymermelt;Polymers;Rheometry;Shearmodulus;Testing;Viscositymeasurement
【摘要】:ThispartofISO6721specifiesthegeneralprinciplesofamethodfordeterminingthedynamicrheologicalpropertiesofpolymermeltsatangularfrequenciestypicallyintherange0,01rad·sto100rad·sbymeansofanoscillatoryrheometerwithaparallel-plategeometry.Angularfrequenciesoutsidethisrangecanalsobeused(seenote1).Themethodisusedtodeterminevaluesofthefollowingdynamicrheologicalproperties:complexshearviscosityη,dynamicshearviscosityη',theout-of-phasecomponentofthecomplexshearviscosityη",complexshearmodulusG,shearlossmodulusG"andshearstoragemodulusG'.Itissuitableformeasuringcomplexshearviscosityvaluestypicallyuptoapproximately10MPa·s(seenote2).NOTE1Theangular-frequencymeasurementrangeislimitedbythespecificationofthemeasuringinstrumentandalsobytheresponseofthespecimen.Whentestingusingangularfrequencieslowerthan0,1rad·sthetesttimecanincreasesignificantlyasthetimetakentoobtainasinglemeasurementisproportionaltothereciprocaloftheangularfrequency.Consequently,whentestingatlowangularfrequenciesdegradationorpolymerizationofthespecimenismorelikelytooccurandhaveaneffectontheresults.Athighangularfrequenciesthespecimenmaydistortorfractureattheedge,consequentlyinvalidatingthetestresults.NOTE2Therangeofcomplexshearviscosityvaluesthatcanbemeasuredisdependentonthespecimendimensionsandalsothespecificationofthemeasuringinstrument.Foraspecimenofgivendimensions,theupperlimitoftherangeislimitedbythemachine'storquecapacity,angular-displacementresolutionandcompliance.However,correctioncanbemadeforcomplianceeffects.
【中国标准分类号】:G31
【国际标准分类号】:83_080_01
【页数】:15P.;A4
【正文语种】:英语
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